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Methyl 3-chloro-4-hydroxyphenylacetate → 3-Chloro-4-(3'-methyl-4'-isopropoxybenzyloxy) phenylacetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 3-chloro-4-hydroxyphenylacetate | HCID 92625 | — |
| 反応物 | 3-Methyl-4-isopropoxybenzyl chloride | HCID 12347937 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 3-Chloro-4-(3'-methyl-4'-isopropoxybenzyloxy) phenylacetic acid | HCID 12347958 | 35.2% |
反応手順
3-chloro-4-(3'-methyl-4'-isopropoxybenzyloxy) phenylacetic acid was prepared in 35.2% yield, m.p. 104°-105° C. (methanol) by reaction of 3-methyl-4-isopropoxybenzyl chloride with methyl 3-chloro-4-hydroxyphenylacetate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04221919 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-d8e0b81e2c234c8b87680ef0a112eb96 |
| 出典メモ | uspto-grants-1980_09 |