化工社化工社 化学情報印刷レポート · 研究参考用
4-Isopropylbenzyl chloride → 3-Chloro-4-(4'-isopropylbenzyloxy) phenylacetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Isopropylbenzyl chloride | HCID 74916 | — |
| 反応物 | Methyl 3-chloro-4-hydroxyphenylacetate | HCID 92625 | — |
| 溶媒 | Methanol--water (1/1) | HCID 22242641 | — |
| 生成物 | 3-Chloro-4-(4'-isopropylbenzyloxy) phenylacetic acid | HCID 51057233 | — |
反応手順
3-chloro-4-(4'-isopropylbenzyloxy) phenylacetic acid was prepared in accordance with the procedure designated (f) above by reacting 4-isopropylbenzyl chloride with methyl 3-chloro-4-hydroxyphenylacetate. The resultant product evidenced a melting point of 146.5°-148° C. in a methanol-water 2:1 mixture.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04221919 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-2f92acfef37b4fc4a8710866b2b3d64a |
| 出典メモ | uspto-grants-1980_09 |