化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → N-cyclooctyl-N-(2-chloroethyl)ammonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 2-(Cyclooctylamino)ethan-1-ol | HCID 13288215 | — |
| 生成物 | N-cyclooctyl-N-(2-chloroethyl)ammonium chloride | HCID 18316362 | — |
反応手順
2-Hydroxyethylamine was reacted with cyclooctyl bromide according to Method B2a to give N-cyclooctyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cyclooctyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 2-methoxy-4-nitrophenyl isothiocyanate to give 2-(2-methoxy-4-nitrophenylimino)-3-cyclooctyl-1,3-thiazolidine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06353006B1 |
| 出典データセット | uspto-grants-2002_03 |
| ORD ID | ord-f687e00a6077460fb2d83b5d4ff83737 |
| 出典メモ | uspto-grants-2002_03 |