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1-Chloro-3-isothiocyanato-2-methylbenzene → 2-(3-Chloro-2-methylphenylimino)-3-(cyclopentylmethyl)-1,3-thiazolidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Chloro-3-isothiocyanato-2-methylbenzene | HCID 140504 | — |
| 反応物 | N-cyclopentylmethyl-N-(2-chloroethyl)ammonium chloride | HCID 18316280 | — |
| 生成物 | 2-(3-Chloro-2-methylphenylimino)-3-(cyclopentylmethyl)-1,3-thiazolidine | HCID 18316239 | — |
反応手順
2-Hydroxyethylamine was reacted with cyclopentylmethyl bromide according to Method B2a to give N-cyclopentylmethyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cyclopentylmethyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 3-chloro-2-methylphenyl isothiocyanate to give 2-(3-chloro-2-methylphenylimino)-3-(cyclopentylmethyl)-1,3-thiazolidine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06353006B1 |
| 出典データセット | uspto-grants-2002_03 |
| ORD ID | ord-df0ac5b64f9d4de38cad3382da8173a3 |
| 出典メモ | uspto-grants-2002_03 |