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1-Isothiocyanato-2-methoxy-4-nitrobenzene → 2-(2-Methoxy-4-nitrophenylimino)-3-(cyclohexylmethyl)-1,3-thiazolidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Isothiocyanato-2-methoxy-4-nitrobenzene | HCID 610837 | — |
| 反応物 | N-cyclohexylmethyl-N-(2-chloroethyl)ammonium chloride | HCID 18316318 | — |
| 生成物 | 2-(2-Methoxy-4-nitrophenylimino)-3-(cyclohexylmethyl)-1,3-thiazolidine | HCID 18316444 | — |
反応手順
2-Hydroxyethylamine was reacted with cyclohexylmethyl bromide according to Method B2a to give N-cyclohexylmethyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cyclohexylmethyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 2-methoxy4-nitrophenyl isothiocyanate to give 2-(2-methoxy-4-nitrophenylimino)-3-(cyclohexylmethyl)-1,3-thiazolidine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06353006B1 |
| 出典データセット | uspto-grants-2002_03 |
| ORD ID | ord-5f227c8ca1db498697b70ac65759e324 |
| 出典メモ | uspto-grants-2002_03 |