Isobutylamine → HCID 18316497、化合物

反応式

[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[N:11]=[C:12]=[S:13].[CH2:14]([NH2:18])[CH:15]([CH3:17])[CH3:16].Cl[CH:20]([CH2:24][CH:25]([CH3:27])[CH3:26])[C:21](O)=[O:22]>>[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[N:11]=[C:12]1[N:18]([CH2:14][CH:15]([CH3:17])[CH3:16])[C:21](=[O:22])[CH:20]([CH2:24][CH:25]([CH3:27])[CH3:26])[S:13]1

参加物

反応物 3

HCID 6558Isobutylamine

HCID 1456212-Methyl-4-nitrophenyl isothiocyanate

HCID 1690712-Chloro-4-methylpentanoic acid

生成物 1

HCID 18316497HCID 18316497、化合物

実験手順

2-Methyl-4-nitrophenyl isothiocyanate was reacted with isobutylamine followed by 2-chloro-4-methylpentanoic acid according to Method C8a to afford 2-(2-methyl-4-nitrophenylimino)-3-isobutyl-5-isobutyl-1,3-thiazolidin-4-one.

出典と根拠

ORDレコード: ord-6e4e4220080e44d9bfb772c36efb5978
出典データセット: uspto-grants-2002_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06353006B1

反応ノート

読み込み中…