反応式
[Cl:1][C:2]1[CH:6]=[CH:5][S:4][C:3]=1B(O)O.ClC1C=CSC=1.Br[C:17]1[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=1>>[Cl:1][C:2]1[CH:6]=[CH:5][S:4][C:3]=1[C:18]1[CH:17]=[CH:22][CH:21]=[CH:20][N:19]=1参加物
4
実験手順
3-Chlorothiophene-2-boronic acid (1.5 g, 9.24 mmol), prepared as described in EXAMPLE 48, Part A from 3-chlorothiophene was reacted with 3-bromopyridine (0.81 mL, 8.4 mmol) as described in EXAMPLE 48, Part B to give the title compound (0.232 g, 1.19 mmol).
出典と根拠
- ORDレコード
- ord-d795401eb6db4990a351bd0a3efc3fc2
- 出典データセット
- uspto-grants-1998_03
- 特許番号
- US05731315
関連ノート
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