Acrylamide → Prop-2-enimidic acid--2-(dimethylamino)ethyl 2-methylprop-2-enoate (1/1)

HRID 27834

反応式

HRID 27834 の反応式
[CH3:1][C:2]([C:4]([O:6][CH2:7][CH2:8][N:9]([CH3:11])[CH3:10])=[O:5])=[CH2:3].[C:12]([NH2:16])(=[O:15])[CH:13]=[CH2:14]>>[C:12]([NH2:16])(=[O:15])[CH:13]=[CH2:14].[CH3:3][C:2]([C:4]([O:6][CH2:7][CH2:8][N:9]([CH3:11])[CH3:10])=[O:5])=[CH2:1]

参加物

3

反応物 2

HCID 6579AcrylamideHCID 17869(Dimethylamino)ethyl methacrylate2 回

生成物 1

HCID 160008Prop-2-enimidic acid--2-(dimethylamino)ethyl 2-methylprop-2-enoate (1/1)

反応条件

温度
85 °C

実験手順

This example demonstrates the effect of reaction temperature on the quat content. Example 9C was repeated except that the temperature was raised to 85° C. before the initiator was added. After 6 hours G.L.C. analysis showed no DMAEMA and no acrylamide present. This indicates that none of the DMAEMA had been quaternized.

後処理

  1. customthe effect of reaction temperature on the quat content
  2. additionwas added

出典と根拠

ORDレコード
ord-b4024651ddb646fda3b64ce73c2962c6
出典データセット
uspto-grants-1980_09
特許番号
US04224150

関連ノート

読み込み中…