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Water → Barium Tridecanephosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Barium(2+) dichloride | HCID 5360350 | — |
| 反応物 | Tridecylphosphonic acid disodium salt | HCID 88784368 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Barium Tridecanephosphonate | HCID 23340094 | 96.3% |
反応手順
Tridecylphosphonic acid disodium salt 123 g (0.4 mole), distilled water 500 ml and ethanol 30 ml were charged into a reaction flask and dissolved by stirring at room temperature. To this solution, 20% barium chloride aq. solution 416 g (0.4 mole) was added and allowed to react for one hour at room temperature. The compound precipitated was filtered off, repeatedly washed with water until free of sodium chloride and dried to obtain 154 g of white powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04224203 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-acf0677b27be4cc5b0219f09973a1e85 |
| 出典メモ | uspto-grants-1980_09 |