化工社化工社 化学情報印刷レポート · 研究参考用
Pivalic acid → n-Neopentanoyl-2-butyloctylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pivalic acid | HCID 6417 | — |
| 反応物 | 2-Butyl-n-octan-1-amine | HCID 18673284 | — |
| 溶媒 | Heptane | HCID 8900 | — |
| 生成物 | n-Neopentanoyl-2-butyloctylamine | HCID 18673286 | 76% |
反応手順
10.4 g of pivalic acid and 17.2 g of 2-butyloctylamine were mixed together in the tube of a microwave machine (Maxidigest™ MX 350 from the company Prolabo; frequency 2450±50 MHz, modulable power 300 W). After irradiation for about 1 hour at 160° C.±10° C., the reaction mixture was dissolved in heptane and then purified on silica. 19 g of the desired amide were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06359175B1 |
| 出典データセット | uspto-grants-2002_03 |
| ORD ID | ord-8b27d062e00d4dcfacb35b68adc53cff |
| 出典メモ | uspto-grants-2002_03 |