化工社化工社 化学情報印刷レポート · 研究参考用
3,5,5-Trimethylhexanoic acid → n-(3,5,5-Trimethylhexanoyl)-2-butyloctylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5,5-Trimethylhexanoic acid | HCID 90960 | — |
| 反応物 | 1400w Dihydrochloride | HCID 2733515 | — |
| 反応物 | 2-Butyl-n-octan-1-amine | HCID 18673284 | — |
| 溶媒 | Heptane | HCID 8900 | — |
| 生成物 | n-(3,5,5-Trimethylhexanoyl)-2-butyloctylamine | HCID 18673287 | 77% |
反応手順
29.2 g of 3,5,5-trimethylhexanoic acid and 34.2 g of 2-butyloctylamine were mixed together in an open Pyrex container and placed in a microwave oven (Menumaster™3100 i; frequency 2450, power at a setting of 30%: 1400 W). After 6 irradiations of about 5 minutes (for each irradiation), the reaction mixture was dissolved in heptane and then purified on silica. 46 g (77%) of the desired amide were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06359175B1 |
| 出典データセット | uspto-grants-2002_03 |
| ORD ID | ord-5fb2aa7435834a2a9de928fec37e62b3 |
| 出典メモ | uspto-grants-2002_03 |