関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 16-Methylheptadecanoic Acid | HCID 21859 | — |
| 生成物 | HCID 56636674 | HCID 56636674 | 5,000% |
反応手順
To 32 g (0.1 mole) of isostearic acid there is added 0.3 ml (0.002 mole) of triethylamine. The resulting mixture is heated to 130° C. under a nitrogen atmosphere and there are slowly added thereto 40 g (0.1 mole) of 2-octyl dodecyl ether of glycidyl obtained according to the above method. After heating for 3 hours and 15 minutes at 130° C., the amount of the reaction determined by acid index is 93%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04224311 |
|---|
| 出典データセット | uspto-grants-1980_09 |
|---|
| ORD ID | ord-2dc269c23b514a9789547f511597a9fb |
|---|
| 出典メモ | uspto-grants-1980_09 |
|---|
