化工社化工社 化学情報印刷レポート · 研究参考用
1,8-Diaminonaphthalene → 2-(m-trifluoromethylphenyl)-1H-perimidine hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,8-Diaminonaphthalene | HCID 68067 | — |
| 反応物 | 3-(Trifluoromethyl)benzoyl chloride | HCID 75257 | — |
| 生成物 | 2-(m-trifluoromethylphenyl)-1H-perimidine hydrochloride | HCID 12945437 | 95.4% |
反応手順
1,8-Diaminonaphthalene (15.82 g.; 0.10 mole) and m-trifluoromethylbenzoyl chloride (20.8 g.; 0.10 mole) were reacted in the same procedures as reported in Example 1, yielding 33.3 g. (95.4% yield) of 2-(m-trifluoromethylphenyl)-1H-perimidine hydrochloride, m.p. 280° C. (dec), mass spectrum m/e 312.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04224326 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-49d57511993d4538a36b4d6ba6c28f34 |
| 出典メモ | uspto-grants-1980_09 |