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Benzoyl fluoride, 4-(trifluoromethoxy)- → 2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoyl fluoride, 4-(trifluoromethoxy)- | HCID 67612 | — |
| 反応物 | 1,8-Diaminonaphthalene | HCID 68067 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE | HCID 12945439 | — |
反応手順
1,8-Diaminonaphthalene (1.52 grams; 0.0096 mole) was dissolved in 25 ml. of toluene, then decanted. p-Trifluoromethoxybenzoyl fluoride (2.0 grams; 0.0096 mole) was dissolved in 25 ml. of toluene. Both solutions were added simultaneously to 25 ml. of toluene. After the reaction mixture had been stirred for approximately 4 hours, TLC indicated that the reaction was complete.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04224326 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-ef9f817d260c40a48ed57129ebeb83cc |
| 出典メモ | uspto-grants-1980_09 |