化工社化工社 化学情報印刷レポート · 研究参考用
3-(Trifluoromethyl)aniline → 3-oxo-N-[3-(trifluoromethyl)phenyl]butanamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(Trifluoromethyl)aniline | HCID 7375 | — |
| 反応物 | Diketene | HCID 12661 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 3-oxo-N-[3-(trifluoromethyl)phenyl]butanamide | HCID 744366 | — |
反応手順
m-Trifluoromethyl aniline (32.22 g) in benzene was dissolved in benzene and diketene added slowly with mixing. The reaction mixture was allowed to stand at 25° C. The resulting solid product was recrystallized from ethanol to yield 3'-trifluoromethyl acetoacetanilide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04224334 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-e2e79f9094af4c188695b3e1de86223b |
| 出典メモ | uspto-grants-1980_09 |