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8-Hydroxyquinoline → Zinc oxyquinolate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 8-Hydroxyquinoline | HCID 1923 | — |
| 反応物 | Zinc acetate (USP) | HCID 2724192 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Zinc oxyquinolate | HCID 84127 | 89.4% |
反応手順
Zinc acetate dihydrate (1.0 g) was dissolved in 75 ml. of hot methanol and 1.4 g of 8-hydroxyquinoline was added to the homogeneous solution. A yellow precipitate formed after a few minutes and the solution was stirred at reflux for 3 hours. The solution was allowed to cool and the precipitate was isolated by filtration and washed with methanol and petroleum ether. After air drying, 1.44 g of bis(8-hydroxyquinolinato)zinc was obtained as a bright yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06362339B1 |
| 出典データセット | uspto-grants-2002_03 |
| ORD ID | ord-abc429fc50e549d38327d32c4b5108cd |
| 出典メモ | uspto-grants-2002_03 |