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Methyl carbazate → N-(methoxycarbonyl)-N'-(2-benzylcyclohexylidene)-hydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl carbazate | HCID 80519 | — |
| 反応物 | 2-Benzylcyclohexan-1-one | HCID 98945 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-(methoxycarbonyl)-N'-(2-benzylcyclohexylidene)-hydrazine | HCID 57106415 | 96.9% |
反応手順
18.83 g (0.1 mole) of 2-benzylcyclohexan-1-one and 9.0 g (0.1 mole) of N-methoxycarbonyl hydrazine are dissolved in 100 cm3 of anhydrous ethanol, and the solution is boiled for 2 hours. Then it is cooled, and the separated crystals are filtered off. 18.2 g (96.9%) of the named compound are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04587261 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-22f0f84b0feb478f8e647024c2ae3d75 |
| 出典メモ | uspto-grants-1986_05 |