化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → D-Ribopyranosyl amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | Ammonium Chloride | HCID 25517 | — |
| 反応物 | Aldehydo-D-ribose | HCID 5311110 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | D-Ribopyranosyl amine | HCID 54279899 | 932.5% |
反応手順
To 100 ml of methanol was added 20 g of D-ribose and 0.5 g of ammonium chloride. This mixture was treated with anhydrous ammonia at 0° C. until a solution was obtained. This solution was stored at 0° C. for 13 days, then the solid was collected, giving 13 g of D-ribopyranosylamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04587331 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-6c82f99df2f64048a4c2ef165cd553e6 |
| 出典メモ | uspto-grants-1986_05 |