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HRID 279933作成日:2026年10月26日

Guanidine → 2-Amino-4-methoxy-6-methyl-1,3,5-triazine

https://huagongshe.com/reaction/279933

反応式

関与物質

役割名称HCID仕込み量
反応物GuanidineHCID 3520—
反応物1,3,5-Triazin-2-amineHCID 20077—
反応物O-MethylisoureaHCID 75544—
生成物2-Amino-4-methoxy-6-methyl-1,3,5-triazineHCID 15466—
生成物O-MethylisoureaHCID 75544—

反応手順

According to U.S. Pat. No. 3,754,547, 2-amino-s-triazine derivatives can be prepared by reaction of N-cyanimido-esters with guanidine, O-methylisourea or amides. This process is also unsuitable on an industrial scale, since the yields produced are only about one-half of the desired yield (a maximum yield of 45% results in the case of the important compound 2-amino-4-methoxy-6-methyl-s-triazine), and the free O-methylisourea base, which is relatively unstable, must be used as the starting substance in this process.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04587337
出典データセットuspto-grants-1986_05
ORD IDord-0e24c445cce340e38a86658ee8b286ff
出典メモuspto-grants-1986_05