化工社化工社 化学情報印刷レポート · 研究参考用
S-sec-butyl ethylphosphonotrithioic acid → 2-Butanethiol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | S-sec-butyl ethylphosphonotrithioic acid | HCID 13564051 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 2-Butanethiol | HCID 10560 | — |
| 生成物 | Phosphenodithioic ethane | HCID 16131073 | — |
反応手順
Following the procedure as shown in Example 1, step (a), 14.67 g (94%) of the triethylamine salt of S-sec-butyl ethylphosphonotrithioic acid was obtained from 6.0 g (0.0242 mole) of ethylthionophosphine sulfide, 5.80 ml (4.58 g, 0.0508 mole) of sec-butyl mercaptan, and 7.1 ml (5.14 g, 0.0508 mole) of triethylamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04588714 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-8e63865f0003448689fe7282a09d16c0 |
| 出典メモ | uspto-grants-1986_05 |