化工社化工社 化学情報印刷レポート · 研究参考用
1,1'-Carbonyldiimidazole → 5-Pyrimidyl carboxylic acid imidazolide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| 反応物 | Pyrimidine-5-carboxylic acid | HCID 78346 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 5-Pyrimidyl carboxylic acid imidazolide | HCID 86739966 | — |
反応手順
5-pyrimidyl carboxylic acid, 1.9 gm, was added to 30 ml of methylene chloride. 2.4 gm of carbonyldiimidazole was added to the system. The system was stirred at room temperature for 3 hours to form the 5-pyrimidyl carboxylic acid imidazolide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04588735 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-45c587997494432c87f23050fd22982c |
| 出典メモ | uspto-grants-1986_05 |