化工社化工社 化学情報印刷レポート · 研究参考用
Phenylglyoxal → N-(2-(4-Methylphenyl)ethyl)-2-hydroxy-2-phenylethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenylglyoxal | HCID 14090 | — |
| 反応物 | p-Methylphenethylamine | HCID 76751 | — |
| 反応物 | 3-(Trifluoromethyl)phenylglyoxal | HCID 2783284 | — |
| 生成物 | N-(2-(4-Methylphenyl)ethyl)-2-hydroxy-2-phenylethanamine | HCID 23322154 | — |
反応手順
The title compound was prepared in the manner described in Example 9, replacing 2-(4-methylphenyl)-1,1-dimethylethanamine by 2-(4-methylphenyl)ethanamine and 3-trifluoromethylphenylglyoxal by phenylglyoxal. The chromatographed material was recrystallised from hexane to give the title compound, mp 95°-97°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04588749 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-2b3502e5393e4644bdebfb3df05b7ba9 |
| 出典メモ | uspto-grants-1986_05 |