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Methanol → D-Tyrosine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Water | HCID 962 | — |
| 反応物 | L-Tyrosine | HCID 6057 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | D-Tyrosine | HCID 71098 | — |
反応手順
Example 1 was repeated with the difference that the sample to be tested was a tyrosine of unknown enantiomer composition, the comparison samples were (RS)-, (R)-, and (S)-tyrosine, and the mobile phase was a mixture of methanol, water, and acetonitrile in a 1:1:0.6 ratio by volume. In this case, the (R)-tyrosine gave a spot with an Rf -value of 0.34 and the (S)-tyrosine gave a spot with an Rf value of 0.26.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04590167 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-b797c9bf619347f691fe461e33ed48fa |
| 出典メモ | uspto-grants-1986_05 |