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HRID 280723作成日:2026年10月26日

M-Cresol → 2,4,6-Trimethylphenol

https://huagongshe.com/reaction/280723

反応式

関与物質

役割名称HCID仕込み量
反応物M-CresolHCID 342—
反応物P-CresolHCID 2879—
反応物Dimethyl EtherHCID 8254—
反応物2,3,6-TrimethylphenolHCID 17016—
溶媒MethanolHCID 887—
生成物2,4,6-TrimethylphenolHCID 10698—

反応手順

methylating meta-cresol and para-cresol in the ortho position by reacting the meta-cresol and para-cresol with methanol, dimethyl ether or a mixture thereof at a temperature of 270° to 450° C., at a pressure of atmospheric to 100 bar and in the presence of a catalyst bed without a residence time of 0.01 to 10 seconds, whereby a mixture of 2,3,6-trimethylphenol and 2,4,6-trimethylphenol is produced;

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04590306
出典データセットuspto-grants-1986_05
ORD IDord-1fec35ca492647bfab2337bac42a837c
出典メモuspto-grants-1986_05