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Benzyl Chloride → Methylbis(phenylmethyl)benzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Chloride | HCID 7503 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Methylbis(phenylmethyl)benzene | HCID 3034397 | 61.3% |
反応手順
To a reaction vessel were added 2500 g of toluene and 50 g of FeCl3 and reaction was carried out for 3 hours by adding 1500 g of benzyl chloride with stirring at room temperature. After the reaction, the catalyst was deactivated and 660 g of dibenzyltoluene was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04591948 |
| 出典データセット | uspto-grants-1986_05 |
| ORD ID | ord-ebea58e4aaa9401d84cda982d468cbbe |
| 出典メモ | uspto-grants-1986_05 |