Benzyl Chloride → Methylbis(phenylmethyl)benzene

HRID 280989

反応式

HRID 280989 の反応式
[CH2:1](Cl)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C1(C)C=CC=CC=1>[CH2:1]([C:3]1[C:2]([CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[C:7]([CH3:1])[CH:6]=[CH:5][CH:4]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

参加物

3

反応物 1

HCID 7503Benzyl Chloride

生成物 1

HCID 3034397Methylbis(phenylmethyl)benzene収率 61.3%

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

To a reaction vessel were added 2500 g of toluene and 50 g of FeCl3 and reaction was carried out for 3 hours by adding 1500 g of benzyl chloride with stirring at room temperature. After the reaction, the catalyst was deactivated and 660 g of dibenzyltoluene was obtained.

後処理

  1. additionTo a reaction vessel were added
  2. customAfter the reaction

出典と根拠

ORDレコード
ord-ebea58e4aaa9401d84cda982d468cbbe
出典データセット
uspto-grants-1986_05
特許番号
US04591948

関連ノート

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