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3-Bromothiophene → 1-(2,4-Dimethyl-5-oxazolyl)-1-(3-thienyl)propanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Bromothiophene | HCID 13383 | — |
| 反応物 | 2,4-Dimethyl-5-propionyloxazole | HCID 18936323 | — |
| 生成物 | 1-(2,4-Dimethyl-5-oxazolyl)-1-(3-thienyl)propanol | HCID 18936368 | — |
反応手順
Starting with 3-bromothiophene and 2,4-dimethyl-5-propionyloxazole and following the general method of Example 4 the title compound was prepared. Purification by preparative HPLC gave a white solid. M.p. 81°-83° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05731335 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-8c46d271dc924094b2300f23ad9e41d8 |
| 出典メモ | uspto-grants-1998_03 |