化工社化工社 化学情報印刷レポート · 研究参考用
Diethylamine → Acetoacetamide, N,N-diethyl-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethylamine | HCID 8021 | — |
| 反応物 | Ethyl Acetoacetate | HCID 8868 | — |
| 生成物 | Acetoacetamide, N,N-diethyl- | HCID 16699 | 65.7% |
反応手順
40 g (0.31 mol) of ethyl acetoacetate and 24 g (0.33 mol) of diethylamine were stirred in a Parr apparatus at 150° C. for 10'. The crude mixture was distilled at 115°-120° C./9 mmHg, to give 32 g of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05731322 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-51c44092234a4bbebe6940b7ac132c46 |
| 出典メモ | uspto-grants-1998_03 |