化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl Acetoacetate → 3-Oxo-n,n-dipropylbutanamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Acetoacetate | HCID 8868 | — |
| 反応物 | Dipropylamine | HCID 8902 | — |
| 生成物 | 3-Oxo-n,n-dipropylbutanamide | HCID 249207 | 0.6% |
反応手順
43.4 g (43.3 mol) of ethyl acetoacetate and 33.7 g (43.3 mol) of dipropylamine were treated as described in preparation 1. The crude oil was distilled at 86°-89° C./ 0.8 mmHg, to give 44.3 g of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05731322 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-9d861ba9b54b4ef8a7a1d9b237766965 |
| 出典メモ | uspto-grants-1998_03 |