化工社化工社 化学情報印刷レポート · 研究参考用
Water → HCID 178418442、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Benzenediazonium chloride | HCID 60992 | — |
| 反応物 | 3-Oxo-n,n-dipropylbutanamide | HCID 249207 | — |
| 反応物 | HCID 178418247 | HCID 178418247 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 178418442 | HCID 178418442 | 14.5% |
反応手順
18.5 g (0.1 mol) of N,N-dipropyl-3-oxobutyramide, 12 g (0.146 mol) of CH3COONa, 20 ml of water, 75 ml of ethanol and a solution of 0.1 mol of phenyldiazonium chloride were treated as described in preparation 2. The precipitated solid was filtered and dried in vacuo yielding 4.2 g of the title compound. M.p.=79°-80° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05731322 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-549c90cb2eaf4302a24586469500c664 |
| 出典メモ | uspto-grants-1998_03 |