化工社化工社 化学情報印刷レポート · 研究参考用
Acetoacetanilide → HCID 178418293、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetoacetanilide | HCID 7592 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Benzenediazonium chloride | HCID 60992 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178418293 | HCID 178418293 | 47.6% |
反応手順
4.5 g (25.4 mmol) of acetoacetanilide, a solution of 3.46 g (89 mmol) of NaOH in 45 ml of water and 95 mmol of phenyldiazonium chloride were treated as described in preparation 8. The residue was crystallised from EtOH, yielding 3.4 g of the title compound. M.p.=96°-97° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05731322 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-f388a24479e44c98bc290884466e1ad3 |
| 出典メモ | uspto-grants-1998_03 |