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HRID 28715作成日：2026年10月26日

2-Fluorobenzenesulphonyl chloride → N-(6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-2-fluorobenzenesulfonamide

https://huagongshe.com/reaction/28715

反応式

関与物質

役割名称HCID仕込み量
反応物2-Fluorobenzenesulphonyl chlorideHCID 137761—
反応物6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amineHCID 597879—
生成物N-(6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-2-fluorobenzenesulfonamideHCID 11407576—

反応手順

N-(6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-2-fluorobenzenesulfonamide was prepared from 2-fluorobenzenesulfonylchloride and 6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine in a similar manner as described above to give a white solid: 1H-NMR (CDCl3): δ 8.56 (s, 1H), 8.00 (m, 1H), 7.65 (m, 1H), 7.58 (m, 1H), 7.2-7.4 (m, 3H), 5.04 (d, 1H), 4.60 (m, 1H), 2.65 (m, 2H), 1.6-2.1 (m, 4H); MS m/z 421 (M−1).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07419997B2
出典データセットuspto-grants-2008_09
ORD IDord-6933d37e757745a6994184f4f46e407e
出典メモuspto-grants-2008_09