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4-(Trifluoromethyl)benzylamine → 3-chlorophenyl-2-(1-hydroxycyclohexyl)-N-[4-(trifluoromethyl)benzyl]acetamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Trifluoromethyl)benzylamine | HCID 76804 | — |
| 反応物 | (3-Chlorophenyl)(1-hydroxycyclohexyl)acetic acid | HCID 68853928 | — |
| 生成物 | 3-chlorophenyl-2-(1-hydroxycyclohexyl)-N-[4-(trifluoromethyl)benzyl]acetamide | HCID 68853662 | — |
反応手順
In an analogous manner to Example 1, step 1 2-(3-chlorophenyl-2-(1-hydroxycyclohexyl)-N-[4-(trifluoromethyl)benzyl]acetamide was prepared from (3-chlorophenyl)(1-hydroxycyclohexyl)acetic acid (Reference Example 1-a) and 4-trifluoromethylbenzylamine. MS (ESI) m/z 426/428 ([M+H]+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07419980B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-8d3110dfd2bf4e63817e96aa0027f33d |
| 出典メモ | uspto-grants-2008_09 |