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Methyl Acetate → {3-[2-(2,4-Dichloro-benzoyl)3-methyl-benzofuran-6-yl]-phenyl}-acetic acid methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl Acetate | HCID 6584 | — |
| 反応物 | (6-Bromo-3-methyl-benzofuran-2-yl)(2,4-dichloro-phenyl)methanone | HCID 59788907 | — |
| 生成物 | {3-[2-(2,4-Dichloro-benzoyl)3-methyl-benzofuran-6-yl]-phenyl}-acetic acid methyl ester | HCID 59788899 | — |
反応手順
{3-[2-(2,4-Dichloro-benzoyl)-3-methyl-benzofuran-6-yl]-phenyl}-acetic acid methyl ester was prepared via a Suzuki coupling of (6-Bromo-3-methyl-benzofuran-2-yl)-(2,4-dichloro-phenyl)-methanone and 3-Bromo-phenyl)-acetic acid methyl ester as described in method 1 step 5. MS ES (MH+)453.1, RT=4.27 min).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07420066B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-a588b0422ee0410ab0ab9e31a6bd2112 |
| 出典メモ | uspto-grants-2008_09 |