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p-(Trifluoromethoxy)benzenesulphonyl chloride → N-[4-Chloro-2-(2-methyl-pyridine-3-carbonyl)-phenyl]-4-trifluoromethoxy-benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-(Trifluoromethoxy)benzenesulphonyl chloride | HCID 523102 | — |
| 反応物 | (2-Amino-5-chloro-phenyl)-(2-methyl-pyridin-3-yl)-methanone | HCID 22327321 | — |
| 生成物 | N-[4-Chloro-2-(2-methyl-pyridine-3-carbonyl)-phenyl]-4-trifluoromethoxy-benzenesulfonamide | HCID 10254153 | — |
反応手順
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using (2 amino-5-chloro-phenyl)-(2-methyl-pyridin-3-yl)-methanone and 4-trifluoromethoxy-benzenesulfonyl chloride and purified by HPLC.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07420055B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-80d24bcdb7734cbdb48ff6dc4306d301 |
| 出典メモ | uspto-grants-2008_09 |