4-t-Butylbenzenesulfonyl chloride → 4-tert-Butyl-N-[4-chloro-2-(1-methyl-1H-imidazole-2-carbonyl)-phenyl]-benzenesulfonamide

HRID 29618

反応式

HRID 29618 の反応式
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S:11](Cl)(=[O:13])=[O:12])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[NH2:15][C:16]1[CH:21]=[CH:20][C:19]([Cl:22])=[CH:18][C:17]=1[C:23]([C:25]1[N:26]([CH3:30])[CH:27]=[CH:28][N:29]=1)=[O:24]>>[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S:11]([NH:15][C:16]2[CH:21]=[CH:20][C:19]([Cl:22])=[CH:18][C:17]=2[C:23]([C:25]2[N:26]([CH3:30])[CH:27]=[CH:28][N:29]=2)=[O:24])(=[O:13])=[O:12])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2]

参加物

3

反応物 2

HCID 1398824-t-Butylbenzenesulfonyl chlorideHCID 10998977(2-amino-5-chlorophenyl)(1-methyl-1H-imidazol-2-yl)methanone

生成物 1

HCID 597887744-tert-Butyl-N-[4-chloro-2-(1-methyl-1H-imidazole-2-carbonyl)-phenyl]-benzenesulfonamide

実験手順

The title compound was prepared using 4-t-butyl-benzenesulfonyl chloride and (2-Amino-5-chloro-phenyl)-(1-methyl-1H-imidazol-2-yl)-methanone following the general procedure described for the preparation of N-aryl-benzenesulfonamides. MS: m/z 452.1 (M++1).

出典と根拠

ORDレコード
ord-53fd5a0702e64a17ba087ca29d079c44
出典データセット
uspto-grants-2008_09
特許番号
US07420055B2

関連ノート

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