関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1,3-Dibromopropane | HCID 8001 | — |
| 反応物 | Diisopropylethylamine | HCID 81531 | — |
| 反応物 | Dimethyl Iminodiacetate Hydrochloride | HCID 2727727 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Dimethyl N-(3-Bromopropyl)iminodiacetate | HCID 19688438 | — |
反応手順
A mixture of 1 mmol iminodiacetic acid dimethylester hydrochloride salt, 5 mmol N,N-diisopropyl-ethylamine and 3 mmol 1,3-dibromopropane in 2 mL toluene was stirred at 90° C. for 16 h and then chromatographed to provide the title compound as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05731432 |
|---|
| 出典データセット | uspto-grants-1998_03 |
|---|
| ORD ID | ord-53859d19f5084c73a9229630dac0c84d |
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| 出典メモ | uspto-grants-1998_03 |
|---|
