関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | p-Fluoronitrobenzene | HCID 9590 | — |
| 反応物 | 2,4-Dimethylbenzene-1,3-diamine | HCID 4625581 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | 4-nitro-N-(3-{[(4-nitrophenyl)amino]methyl}benzyl)aniline | HCID 58794783 | — |
反応手順
1.73 g of para-fluoronitrobenzene (2 eq.) were dissolved in 5 ml of DMSO. 1.2 equivalents of m-xylenediamine and 4 equivalents of triethylamine were added to the solution. The reaction mixture was heated at 60° C. for 20 hours. The mixture was then poured onto crushed ice and a precipitate formed. The latter was filtered, washed with water, and then dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07422609B2 |
|---|
| 出典データセット | uspto-grants-2008_09 |
|---|
| ORD ID | ord-e6dc97c099be42f593855bc0cd045bfe |
|---|
| 出典メモ | uspto-grants-2008_09 |
|---|
