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4-Methoxybenzohydrazide → 4-Methoxy-benzoic acid-(1-imino-propyl)-hydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxybenzohydrazide | HCID 76792 | — |
| 反応物 | Propionimidamide hydrochloride | HCID 12301253 | — |
| 生成物 | 4-Methoxy-benzoic acid-(1-imino-propyl)-hydrazide | HCID 68495483 | — |
反応手順
Prepared from 4.90 g (45 mmol) propioamidine hydrochloride and 5.00 g (30 mmol) 4-methoxy-benzoic acid hydrazide analogously to the procedure laid down for intermediate product 1a). After distillation of the ethanol 10.0 g crude product are obtained, which are reacted without any further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07423036B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-11be8ab7e1c64170894019d1b1ce419a |
| 出典メモ | uspto-grants-2008_09 |