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Trifluoroacetate → 1,1-Dimethyl-3-[5-methyl-3-(4-trifluoromethyl-phenyl)-[1,2,4]triazol-1-yl]-propylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trifluoroacetate | HCID 84468 | — |
| 反応物 | Tert-butyl {1,1-dimethyl-3-[5-methyl-3-(4-trifluoromethyl-phenyl)-[1,2,4]triazol-1-yl]-propyl}-carbamate | HCID 86607261 | — |
| 生成物 | 1,1-Dimethyl-3-[5-methyl-3-(4-trifluoromethyl-phenyl)-[1,2,4]triazol-1-yl]-propylamine | HCID 59789265 | — |
反応手順
Prepared according to the method described for intermediate product 1d) from tert-butyl {1,1-dimethyl-3-[5-methyl-3-(4-trifluoromethyl-phenyl)-[1,2,4]triazol-1-yl]-propyl}-carbamate. White solid. Yield: 4.72 g (trifluoroacetate); mass spectroscopy [M+H]+=313.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07423036B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-cf6b2bf3d5e743049f754a829033340b |
| 出典メモ | uspto-grants-2008_09 |