化工社化工社 化学情報印刷レポート · 研究参考用
1-(Bromomethyl)-4-(trifluoromethyl)benzene → 2-(3,5-Dichlorophenyl)-4-isopropyl-6-{[4-(trifluoromethyl)benzyl]oxy}pyrimidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(Bromomethyl)-4-(trifluoromethyl)benzene | HCID 123062 | — |
| 反応物 | HCID 178439458 | HCID 178439458 | — |
| 生成物 | 2-(3,5-Dichlorophenyl)-4-isopropyl-6-{[4-(trifluoromethyl)benzyl]oxy}pyrimidine | HCID 10366005 | — |
反応手順
The title compound was prepared from 2-(3,5-dichloro-phenyl)-6-isopropyl-pyrimidin-4-ol (which was obtained in Intermediate 6) and 4-(trifluoromethyl)benzyl bromide according to Method A; LC retention time 4.57 min; MS: m/z (ESI) 441 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07423044B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-50b5ce710744452aac637dd3582d1cd2 |
| 出典メモ | uspto-grants-2008_09 |