Veratroyl chloride → 2-(3,4-Dimethoxybenzoyl)-5-methoxybenzoic acid

反応式

[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6](Cl)=[O:7].Br[C:15]1[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][C:16]=1[C:17]([OH:19])=[O:18]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6]([C:15]1[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][C:16]=1[C:17]([OH:19])=[O:18])=[O:7]

参加物

反応物 2

HCID 77070Veratroyl chloride

HCID 899062-Bromo-5-methoxybenzoic acid

生成物 1

HCID 692141502-(3,4-Dimethoxybenzoyl)-5-methoxybenzoic acid

実験手順

This compound is obtained according to the procedure described in 1.1. by reacting 3,4-dimethoxybenzoyl chloride and 2-bromo-5-methoxybenzoic acid after halogen-lithium exchange. It is used in crude form in the following reaction.

後処理

customThis compound is obtained
customin the following reaction

出典と根拠

ORDレコード: ord-e3960857a0f8439392478298ee564953
出典データセット: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07423030B2

反応ノート

読み込み中…

参加物