p-Anisoyl chloride → 2-(4-Methoxybenzoyl)-5-methylbenzoic acid

反応式

[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7](Cl)=[O:8])=[CH:5][CH:4]=1.Br[C:13]1[CH:21]=[CH:20][C:19]([CH3:22])=[CH:18][C:14]=1[C:15]([OH:17])=[O:16]>>[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([C:13]2[CH:21]=[CH:20][C:19]([CH3:22])=[CH:18][C:14]=2[C:15]([OH:17])=[O:16])=[O:8])=[CH:5][CH:4]=1

参加物

反応物 2

HCID 7477p-Anisoyl chloride

HCID 2280802-Bromo-5-methylbenzoic acid

生成物 1

HCID 692118002-(4-Methoxybenzoyl)-5-methylbenzoic acid

実験手順

This compound is obtained according to the procedure described in 1.1. by reacting 4-methoxybenzoyl chloride and 2-bromo-5-methylbenzoic acid after halogen-lithium exchange. It is used in crude form in the following reaction.

後処理

customThis compound is obtained
customin the following reaction

出典と根拠

ORDレコード: ord-42bdeafb19fa4f718e1042462480da8c
出典データセット: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07423030B2

反応ノート

読み込み中…