Phosphorus oxychloride → 1-Chloro-4-ethyl-7-methoxyphthalazine

反応式

[CH2:1]([C:3]1[C:12]2[C:7](=[CH:8][C:9]([O:13][CH3:14])=[CH:10][CH:11]=2)[C:6](=O)[NH:5][N:4]=1)[CH3:2].P(Cl)(Cl)([Cl:18])=O>>[Cl:18][C:6]1[C:7]2[C:12](=[CH:11][CH:10]=[C:9]([O:13][CH3:14])[CH:8]=2)[C:3]([CH2:1][CH3:2])=[N:4][N:5]=1

参加物

反応物 2

HCID 24813Phosphorus oxychloride

HCID 576917044-ethyl-7-methoxy-2H-phthalazin-1-one

生成物 1

HCID 576917031-Chloro-4-ethyl-7-methoxyphthalazine

実験手順

This compound is obtained according to the procedure described in 1.3. by reacting 4-ethyl-7-methoxy-2H-phthalazin-1-one with phosphoryl chloride.

後処理

customThis compound is obtained

出典と根拠

ORDレコード: ord-3bb070770c5c4ed2a895bf8e65ba2ce6
出典データセット: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07423030B2

反応ノート

読み込み中…