化工社化工社 化学情報印刷レポート · 研究参考用
2-Bromo-5-chlorobenzoic acid → 5-chloro-2-(4-methoxybenzoyl)benzoic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromo-5-chlorobenzoic acid | HCID 89027 | — |
| 反応物 | N,4-Dimethoxy-N-methylbenzamide | HCID 15105748 | — |
| 反応物 | Butyllithium | HCID 178418339 | — |
| 生成物 | 5-chloro-2-(4-methoxybenzoyl)benzoic Acid | HCID 11380746 | — |
反応手順
This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-chlorobenzoic acid pretreated with n-butyllithium with 4-methoxy-N-methoxy-N-methyl-benzamide. It is used in crude form in the following reaction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07423030B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-6eb27124c1a34a0e8db0b4628617f14a |
| 出典メモ | uspto-grants-2008_09 |