2-Bromo-5-methoxybenzoic acid → HCID 69212695、化合物

HRID 30058ノート

反応式

HRID 30058 の反応式
Br[C:2]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].C([Li])CCC.[CH2:18]([O:25][CH2:26][C:27](N(OC)C)=[O:28])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH2:18]([O:25][CH2:26][C:27]([C:2]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])=[O:28])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

参加物

4

反応物 3

HCID 899062-Bromo-5-methoxybenzoic acidHCID 114584642-(Benzyloxy)-N-methoxy-N-methylacetamideHCID 178418339Butyllithium

生成物 1

HCID 69212695HCID 69212695、化合物

実験手順

This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with 2-benzyloxy-N-methoxy-N-methylacetamide. The product is used in crude form in the following reaction.

後処理

  1. customThis compound is synthesized
  2. customin the following reaction

出典と根拠

ORDレコード
ord-036e2ad68ef74ff1a12901fee284cd6c
出典データセット
uspto-grants-2008_09
特許番号
US07423030B2

反応ノート

読み込み中…