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Ethyl 4-amino-1-piperidinecarboxylate → 4-[6-Amino-5-(2-fluoro-benzoyl)-pyridin-2-ylamino]-piperidine-1-carboxylic acid ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 4-amino-1-piperidinecarboxylate | HCID 100867 | — |
| 反応物 | (2-Amino-6-chloro-pyridin-3-yl)-(2-fluoro-phenyl)-methanone | HCID 58590830 | — |
| 生成物 | 4-[6-Amino-5-(2-fluoro-benzoyl)-pyridin-2-ylamino]-piperidine-1-carboxylic acid ethyl ester | HCID 11661022 | — |
反応手順
The title compound was prepared from (2-Amino-6-chloro-pyridin-3-yl)-(2-fluoro-phenyl)-methanone (Example 7) and ethyl-4-amino-1-piperidine carboxylate (Aldrich) using the procedure described in Step B. Example 6. HRMS, observed: 386.1762, calcd for M+: 386.1754.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07423051B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-0b0a6e779a6f49c4ab9303d399238a7b |
| 出典メモ | uspto-grants-2008_09 |