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4-Fluoroiodobenzene → (2-Amino-6-chloro-pyridin-3-yl)-(4-fluoro-phenyl)-methanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Fluoroiodobenzene | HCID 9605 | — |
| 反応物 | 2-Amino-6-chloro-N-methoxy-N-methyl-nicotinamide | HCID 58590824 | — |
| 生成物 | (2-Amino-6-chloro-pyridin-3-yl)-(4-fluoro-phenyl)-methanone | HCID 58590828 | — |
反応手順
The title compound was prepared from 2-Amino-6-chloro-N-methoxy-N-methyl-nicotinamide (Example 3) and 1-fluoro-4-iodobenzene (Aldrich 99%) using the procedure described in Example 7. HRMS, observed: 250.0314, Calcd for M+: 250.0309.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07423051B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-63e9c089843b45879c1458c9f2b44eb9 |
| 出典メモ | uspto-grants-2008_09 |