化工社化工社 化学情報印刷レポート · 研究参考用
Morpholine → 4-((5-Bromopyridin-3-yl)methyl)morpholine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Morpholine | HCID 8083 | — |
| 反応物 | 5-Bromo-3-pyridinecarboxaldehyde | HCID 2784734 | — |
| 生成物 | 4-((5-Bromopyridin-3-yl)methyl)morpholine | HCID 22390415 | 61% |
反応手順
The title compound was prepared in a similar way as described in Example 18, Step C, using 5-bromo-pyridine-3-carbaldehyde and morpholine. The crude compound was purified (SiO2: 0-3% 2 M NH3 in MeOH/DCM) to provide the title compound (61%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07423147B2 |
| 出典データセット | uspto-grants-2008_09 |
| ORD ID | ord-fa162b65c69e4dc3b185bf027fd7d8b4 |
| 出典メモ | uspto-grants-2008_09 |