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HRID 31004作成日：2026年10月25日

2,2,3,3,3-Pentafluoropropylamine → N-[(S)-5-(2-Benzyloxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-N'-(2,2,3,3,3-pentafluoro-propyl)-malonamide

https://huagongshe.com/reaction/31004

反応式

関与物質

役割名称HCID仕込み量
反応物2,2,3,3,3-PentafluoropropylamineHCID 79002—
反応物N-[(S)-5-(2-benzyloxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-malonamic acidHCID 58972481—
生成物N-[(S)-5-(2-Benzyloxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-N'-(2,2,3,3,3-pentafluoro-propyl)-malonamideHCID 58972497—

反応手順

Using N—[(S)-5-(2-benzyloxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-malonamic acid and N-(2,2,3,3,3-pentafluoro-propyl amine, the title compound was prepared in the same manner as example 1c (73%). White solid. MS: m/e=576(M+H+).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07425551B2
出典データセットuspto-grants-2008_09
ORD IDord-8dd64c2a938d4775b30d3f48c02a9bef
出典メモuspto-grants-2008_09